CRSEXP038

=Researchers= Grace Petrecca and Matthew McBride =Objective= =Procedure= =Results= [|CRSEXP038_1inD2O]: Sample #1 mixed in D2O **[This can't be in D2O since there is clearly TMS and chloroform JCB]**

Using co-axial insert with CDCl3 as the reference solvent: [|CRSEXP038_2_16scans]: Sample #2 [|CRSEXP038_3_16scans]: Sample #3 [|CRSEXP038_4_16scans]: Sample #4 [|CRSEXP038_5_16scans]: Sample #5 [|CRSEXP038_6_16scans]: Sample #6
 * Need to get file for Sample #1 from the NMR computer - MJM**

CRSEXP038sheet1

FID Files:

Sample #1: Sample #2: Sample #3: Sample #4: Sample #5: Sample #6: =Discussion= =Conclusion= =Log=
 * [There are definitely some differences between the wines for well defined peaks - check the region 1-4 ppm and 9-10ppm and try to assign which compounds these peaks represent. You will need to use the mole fraction template for this. JCB]]**

2013-11-15
14:00 Analyzed the Wine #1 (CRSEXP038_1inD2O) by 500 MHz HNMR using a traditional NMR tube with the sample mixed in D2O. Analyzed Wine #1-6 by 500 MHz HNMR with the sample in a co-axial insert and CDCl3 in the outer NMR tube. The files for these spectra are the following: CRSEXP038_1_16scans, CRSEXP038_2_16scans, CRSEXP038_3_16scans, CRSEXP038_4_16scans, CRSEXP038_5_16scans and CRSEXP038_6_16scans.