CRSEXP040

Researcher
Kayla Gogarty

Objective
The purpose of this experiment is to determine the results of a reaction of Acetic Anhydride and Phenanthrene-9-Carboxaldehyde, using HNMR to analyze the results.

Results
Time: 30 minutes [|CRSEXP040B HNMR] Acetic Anhydride [|CRSEXP040C HNMR] Few grains of Phenanthrene-9-carboxaldehyde in excess acetic anhydride [|CRSEXP040D HNMR] 1 scoop of Phenanthrene-9-carboxaldehyde with enough acetic acid to dissolve

Time: 24 hours [|CRSEXP040B-2 HNMR] Acetic Anhydride [|CRSEXP040C-2 HNMR] Few grains of Phenanthrene-9-carboxaldehyde in excess acetic anhydride [|CRSEXP040D-2 HNMR] 1 scoop of Phenanthrene-9-carboxaldehyde with enough acetic anhydride to dissolve

Log
15:00pm: Made three mixtures (CRSEXP040B, CRSEXP040C, CRSEXP040D) CRSEXP040B - Acetic Anhydride CRSEXP040C - Few grains of Phenanthrene-9-carboxaldehyde in excess acetic anhydride CRSEXP040D - 1 scoop of Phenanthrene-9-carboxaldehyde with enough acetic acid to dissolve
 * 28 January 2014**

15:30pm: Took HNMR spectra of CRSEXP040B, CRSEXP040C, and CRSEXP040D 16scans, 1s relaxation delay, 45degrees pulse angle, CDCl3 as solvent

16:00pm: Took HNMR spectra CRSEXP040B-2, CRSEXP040C-2, CRSEXP040D-2 16scans, 1s relaxation delay, 45degrees pulse angle, CDCl3 as solvent
 * 29 January 2014**