CRSEXP047

=Researcher= Andrew Buss

=Objective= This experiment had two objectives. 1) To determine if an applied voltage would impart any changes on acetonitrile in the absence of electrolyte, and if so at what voltage threshold. And 2) to determine if the non-inert copper electrodes have any effect on the system.

=Results=

[|CRSEXP046 Pure ACN HNMR] (TMS lock) [|CRSEXP046 Supernatant HNMR] (TMS lock)



= = =Log=

2014-04-28

15:45 0.883g ACN measured in vial for analysis 15:50 Picture 6 taken 16:00 Applied 23.5V and started video 1 [] 16:03 Black residue starting to form 16:10 Black residue increasing 16:21 Power halted and video 1 stopped, picture 7 taken 16:29 Picture 8 taken (<1mg of product recovered) 17:00 NMR 3, 4 taken